J. Lipid Res. Acyl Labeled PIP's available August 1, 2008
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Journal of Lipid Research, Vol. 1, 405-411, October 1960
Copyright © 1960 by Lipid Research, Inc.

Synthesis of enantiomeric mixed-acid agr,ß-diglycerides

Dmytro Buchnea and Erich Baer

Subdepartment of Synthetic Chemistry in Relation to Medical Research, Banting and Best Department of Medical Research University of Toronto, Toronto, Canada

A procedure has been developed that permits the synthesis of mixed-acid agr,ß-diglycerides in either one of the four theoretically possible isomeric forms. Each is obtainable as a pure compound devoid of any contamination with positional or spatial isomers. Their fatty acid substituents may consist either of two dissimilar saturated fatty acids or a saturated and an unsaturated fatty acid. The procedure has been applied to the synthesis of d-agr-stearoyl-ß-oleoylglycerol and d-agr-oleoyl-ß-stearoylglycerol, the first mixed-acid diglycerides to be obtained in enantiomeric form.

Submitted on April 28, 1960


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