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Journal of Lipid Research, Vol. 10, 128-131, January 1969
Copyright © 1969 by Lipid Research, Inc.

Gas-liquid chromatography of dialkyl, alkyl acyl, and diacyl derivatives of glycerol

Randall Wood , W. J. Baumann , Fred Snyder , and H. K. Mangold

Medical Division,* Oak Ridge Associated Universities, Oak Ridge, Tennessee 37830, and the University of Minnesota, The Hormel Institute, Austin, Minnesota 55912

Dialkyl, alkyl acyl, and diacyl glycerols were resolved as trimethylsilyl ethers and as acetates by gas-liquid chromatography on a nonpolar stationary phase (OV-1). The two types of derivatives proved suitable for quantitative gas chromatographic analysis.

Supplementary key words trimethylsilyl ethers • acetates • thin-layer chromatography

Submitted on July 5, 1968
Accepted on September 18, 1968


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