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Journal of Lipid Research, Vol. 10, 465-467, July 1969
Copyright © 1969 by Lipid Research, Inc.

Synthesis and desulfurization-decarboxylation of cyclic thionocarbonates of glycerol 1-ethers

S. Ramachandran , R. V. Panganamala , and David G. Cornwell

Department of Physiological Chemistry, The Ohio State University, Columbus, Ohio 43210

A method is described for the synthesis of cyclic thionocarbonates of 1-O-alkyl glycerols in quantitative yield. These derivatives of glycerol ethers can be quantitated by UV absorbance, analyzed by gas-liquid chromatography, or quantitatively converted to allyl alkyl ethers for gas-chromatographic analysis.

Supplementary key words UV absorbance • gas-liquid • thin-layer • chromatography • mass spectroscopy • allyl alkyl ethers • cyclic carbonate

Submitted on February 11, 1969
Accepted on April 24, 1969


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