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Journal of Lipid Research, Vol. 12, 117-119, January 1971
Copyright © 1971 by Lipid Research, Inc.

Gas-liquid chromatography of hyocholic acid

Glen E. Mott , Richard W. Moore , and Raymond Reiser

Department of Biochemistry and Biophysics, and Department of Veterinary Microbiology, Texas A & M University, College Station, Texas 77843

Partial derivatives of hyocholic acid were formed under the usual conditions for trifluoroacetylation of bile acids (trifluoroacetic anhydride, 35°C for 20 min). Complete trifluoroacetylation of hyocholic acid was achieved at 80°C for 30 min, or at 60°C for 30 min when a trace of pyridine was added to the reaction mixture.

Supplementary key words bile acids • methyl esters • trifluoroacetylation • partial derivatives • steric hindrance • pyridine

Submitted on July 1, 1970
Accepted on October 20, 1970

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