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Journal of Lipid Research, Vol. 12, 636-637, September 1971
Copyright © 1971 by Lipid Research, Inc.

Artifacts produced by boron trifluoride methanolysis of a synthetic lecithin containing cyclopropane fatty acids (1-2-dihydrosterculoyl-3-sn-phosphatidylcholine)

E. A. Dawidowicz and T. E. Thompson

Department of Biochemistry, University of Virginia School of Medicine, Charlottesville, Virginia 22901

It is shown that methanolysis of dihydrosterculoyl lecithin with boron trifluoride-methanol introduces artifacts which are absent if the methyl ester is prepared by saponification of the lipid followed by treatment with diazomethane.

Supplementary key words gas-liquid chromatography • diazomethane

Submitted on February 10, 1971
Accepted on May 12, 1971


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