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Journal of Lipid Research, Vol 18, 404-407, Copyright © 1977 by Lipid Research, Inc.
KY Tserng, DL Hachey and PD Klein
Glycine and taurine conjugates of 5beta-cholanic acids have been
synthesized using improved procedures based on the peptide coupling
reagent, N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline. The conjugates are
obtained in chromatographically pure form in yields higher than 90%. The
use of this procedure in the large scale preparation of
cholyl[1,2-13C2]glycine is described.
ARTICLES
An improved procedure for the synthesis of glycine and taurine conjugates of bile acids
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