J. Lipid Res.
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Journal of Lipid Research, Vol 19, 501-504, Copyright © 1978 by Lipid Research, Inc.

ARTICLES

A convenient synthesis of 3-keto bile acids by selective oxidation of bile acids with silver carbonate-Celite

KY Tserng

A number of 3-keto bile acids were synthesized by the selective oxidation of bile acid methyl esters with silver carbonate-Celite in refluxing toluene. The pure 3-keto bile acids were isolated simply by filtering the reaction mixture and concentrating the filtrate. The relation of the bile acid structure to the oxidation rate is also discussed.
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Copyright © 1978 by the American Society for Biochemistry and Molecular Biology.