J. Lipid Res. Acyl Labeled PIP's available August 1, 2008
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Journal of Lipid Research, Vol 20, 279-284, Copyright © 1979 by Lipid Research, Inc.

ARTICLES

Proton magnetic resonance identification and discrimination of stereoisomers of C27 steroids using lanthanide shift reagents

T Iida, M Kikuchi, T Tamura and T Matsumoto

A simple proton magnetic resonance spectroscopic method is described for the identification and and confirmation of several stereoisomeric paris of C27 stanols as well as their keto and acetate derivatives related to cholesterol. The method, which involves the use of lanthanide shift reagents, is useful in distinguishing clearly between the isomeric pairs differing only in the geometry of a functional group and/or of the A/B-ring junction in the steroid skeleton.
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