J. Lipid Res. Acyl Labeled PIP's available August 1, 2008
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Journal of Lipid Research, Vol 21, 118-122, Copyright © 1980 by Lipid Research, Inc.

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Sterol synthesis. Chemical synthesis of 5 alpha-cholest-7-en-3 beta, 14 alpha-diol

RA Pascal Jr and GJ Schroepfer Jr

Reported herein is the chemical synthesis of 5 alpha-cholest-7-en-3 beta, 14 alpha-diol by mild Wolff-Kishner reduction of 3 beta-acetoxy-8 alpha, 14 alpha-epoxy-5 alpha-cholestan-7-one. The preparation of 5 alpha-cholest-7-en-14 alpha-ol-3-one from 5 alpha is also described. These compounds were fully characterized by the results of infrared, nuclear magnetic resonance, and high and low resolution mass spectral studies.
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G. J. Schroepfer Jr.
Oxysterols: Modulators of Cholesterol Metabolism and Other Processes
Physiol Rev, January 1, 2000; 80(1): 361 - 554.
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