J. Lipid Res. Acyl Labeled PIP's available August 1, 2008
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Journal of Lipid Research, Vol 22, 859-868, Copyright © 1981 by Lipid Research, Inc.

ARTICLES

Sterol synthesis. A simplified method for the synthesis of 32- oxygenated derivatives of 24,25-dihydrolanosterol

EJ Parish and GJ Schroepfer Jr

A simplified method is described for the preparation of 14 alpha- hydroxymethyl-4,4-dimethyl-5 alpha-cholest-8-en-e beta-ol, 14 alpha- hydroxymethyl-4,4-dimethyl-5 alpha-cholest-7-en-3 beta-ol, and 14 alpha- hydroxymethyl-4,4-dimethyl-5-alpha-cholest-6-en-3 beta-ol from commercial lanosterol. This method represents a modification of the approach introduced by Fried and co-workers (Fried, J., J. W. Brown, and L. Borkenhagen. 1965. Tetrahedron Lett. 2499-2504).
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E. S. Kaneshiro, Z. Amit, M. M. Swonger, G. P. Kreishman, E. E. Brooks, M. Kreishman, K. Jayasimhulu, E. J. Parish, H. Sun, S. A. Kizito, et al.
Pneumocysterol [(24Z)-ethylidenelanost-8-en-3beta -ol], a rare sterol detected in the opportunistic pathogen Pneumocystis carinii hominis: Structural identity and chemical synthesis
PNAS, January 5, 1999; 96(1): 97 - 102.
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