J. Lipid Res.
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Journal of Lipid Research, Vol 23, 443-447, Copyright © 1982 by Lipid Research, Inc.

ARTICLES

Preparation of retinoic acid esters of phorbol derivatives

B Sorg, G Furstenberger, DL Berry, E Hecker and F Marks

The synthesis of 12-O-retinoylphorbol-13-acetate (RPA), an incomplete tumor promoter (second stage promoter) is described. The preparation starts with phorbol-13-acetate-20-tritylether which is acylated by a carbodiimide method to yield its 12-retinoate. The latter is detritylated by acidic methanol to give RPA. Following an analogous procedure, the 4-methyl-ether of RPA is prepared from 4-O-methylphorbol- 13-acetate-20-tritylether.
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G Furstenberger, B Sorg, and F Marks
Tumor promotion by phorbol esters in skin: evidence for a memory effect
Science, April 1, 1983; 220(4592): 89 - 91.
[Abstract] [PDF]


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