HOME HELP FEEDBACK SUBSCRIPTIONS ARCHIVE SEARCH TABLE OF CONTENTS		QUICK SEARCH:   [advanced] Author: Keyword(s): Year:  Vol:  Page:

This Article Full Text (PDF) Alert me when this article is cited Alert me if a correction is posted Services Similar articles in this journal Similar articles in PubMed Alert me to new issues of the journal Download to citation manager Request Permissions Citing Articles Citing Articles via Google Scholar Google Scholar Articles by Barua, A. B. Articles by Olson, J. A. Search for Related Content PubMed PubMed Citation Articles by Barua, A. B. Articles by Olson, J. A. Social Bookmarking                      What's this?

Journal of Lipid Research, Vol 26, 258-262, Copyright © 1985 by Lipid Research, Inc.

ARTICLES

Preparation of retinamides by use of retinoyl fluoride

AB Barua and JA Olson

Retinoyl fluoride (2) prepared from retinoic acid (1) by reaction with diethylaminosulfurtrifluoride is a stable crystalline compound not easily hydrolyzed by water. By reacting retinoyl fluoride with water- soluble amines in the presence of sodium bicarbonate, retinamide (4), N- retinoyl glycine (6), N-retinoyl DL-phenylalanine (7), alpha-N-retinoyl- L-lysine (11), N-retinoyl 4-aminophenol (4-hydroxyphenylretinamide) (8), and N-retinoyl-2-amino-2-deoxy-D-glucose (2-deoxy-D-glucose-2- retinamide) (9) have been prepared in good yields and characterized by UV absorption, 1H NMR, IR spectra, mass spectrometry, and elemental analysis.
CiteULike    Complore    Connotea    Del.icio.us    Digg    Reddit    Technorati    What's this?