J. Lipid Res.
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Journal of Lipid Research, Vol 29, 1543-1548, Copyright © 1988 by Lipid Research, Inc.

ARTICLES

Synthesis of 24-heteroatom-substituted cholestanols

MD Rahman, HM Seidel and RA Pascal Jr
Department of Chemistry, Princeton University, NJ 08544.

Short syntheses of 24-thia-5 alpha,20 xi-cholestan-3 beta-ol, 24-methyl- 24-aza-5 alpha,20 xi-cholestan-3 beta-ol, and 24-nor-5 alpha,20 xi- cholan-3 beta-ol from 3 beta-hydroxy-5 alpha-pregnan-20-one are described. The products and synthetic intermediates have been fully characterized by the results of proton NMR, infrared, and high and low resolution mass spectral studies.
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