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Journal of Lipid Research, Vol 30, 127-133, Copyright © 1989 by Lipid Research, Inc.

ARTICLES

Combined in-beam electron impact-B/E-linked scan mass spectrometry of oxazoline derivatives for the structure determination of long-chain unsaturated fatty acids

YM Yang, JY Zhang and ZH Huang
Laboratory of Mass Spectrometry, Shanghai Institute of Materia Medica, Chinese Academy of Sciences.

Long-chain unsaturated fatty acids (UFA) having up to six double bonds are derivatized to 2-substituted 4,4-dimethyloxazolines (DMOX) and then analyzed by combined in-beam electron impact (IBEI)-B/E-linked scan mass spectrometry. This technique provides highly characteristic mass spectra and may serve as an auxiliary means for direct structure determination of individual UFA in mixtures.
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