J. Lipid Res.
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Journal of Lipid Research, Vol 31, 160-162, Copyright © 1990 by Lipid Research, Inc.

ARTICLES

A facile synthesis of [14C] epicholesterol

JS Yan and R Bittman
Department of Chemistry and Biochemistry, Queens College, City University of New York, Flushing 11367.

A facile procedure is described for the preparation of [14C]epicholesterol from [14C]cholesterol. Cholesterol is first converted to cholesteryl mesylate, which is treated with cesium acetate and 18-crown-6 in refluxing toluene to give epicholesteryl acetate. The latter is hydrolyzed, without isolation, with potassium hydroxide in tetrahydrofuran-methanol to give epicholesterol, which is obtained in pure form by preparative thin-layer chromatography.
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