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Journal of Lipid Research, Vol. 7, 422-426, May 1966
Copyright © 1966 by Lipid Research, Inc.

Synthesis and characterization of 3-ketohexadecanoic acid-1-¹⁴C, dl-3-hydroxyhexadecanoic acid-1-¹⁴C, and trans-2-hexadecenoic acid-1-¹⁴C

John A. Jones and Melvin Blecher

Department of Biochemistry, Schools of Medicine and Dentistry, Georgetown University, Washington, D. C.

The chemical synthesis and characterization of three intermediates in the oxidation of palmitic acid-1-¹⁴C by rat liver mitochondria, namely, 3-ketohexadecanoic acid-1-¹⁴C, dl-3-hydroxyhexadecanoic acid-1-¹⁴C, and trans-2-hexadecenoic acid-1-¹⁴C, are described.

Supplementary key words 3-ketohexadecanoic acid-1-¹⁴C • dl-3-hydroxyhexadecanoic acid-1-¹⁴C • trans-2-hexadecenoic acid-1-¹⁴C • synthesis • thin-layer chromatography • IR spectra • intermediates • oxidation • palmitic acid

Submitted on September 21, 1965
Accepted on January 25, 1966

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