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Journal of Lipid Research, Vol. 7, 437-441, May 1966
Copyright © 1966 by Lipid Research, Inc.

Isolation of geranyl geraniol from the unsaponifiable fraction of linseed oil

E. Fedeli , P. Capella , M. Cirimele , and G. Jacini

Stazione Sperimentale per gli Oli e Grassi, Milan, and Centro Nazionale per la Lipochimica del C.N.R., Milan, Italy

From the unsaponifiable fraction (63 g) of linseed oil (25 kg), two terpenic alcohols were isolated by alumina column, thin-layer, and gas-liquid chromatography. They were identified as phytol and geranyl geraniol (a precursor of bi- and tricyclic diterpenes) by infrared and nuclear magnetic resonance spectroscopy, ozonolysis, and mass spectrometry.

Supplementary key words linseed oil • unsaponifiable fraction • phytol • geranyl geraniol • isolation • identification • nuclear magnetic resonance • peanut oil

Submitted on November 23, 1965
Accepted on February 10, 1966


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